Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 466121Generated: October 29, 2026

Acetyl chloride → HCID 14049647, compound

https://huagongshe.com/reaction/466121

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetyl chlorideHCID 6367—
ReactantGimeracilHCID 54679224—
SolventPyridineHCID 1049—
ProductHCID 14049647HCID 1404964752%

Reaction Steps

A 5.00 g quantity of 5-chloro-4-hydroxy-2-pyridone and 3.66 ml of acetyl chloride were stirred in 250 ml of pyridine at room temperature for 3 hours. The reaction mixture was then concentrated and the concentrate was washed with ethyl acetate and water to produce 3.39 g of the title compound in a yield of 52%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05155113
Source datasetuspto-grants-1992_10
ORD IDord-ac4372b4a3d243bcb68fec4e31af3e20
Source noteuspto-grants-1992_10