HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 14049647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Gimeracil | HCID 54679224 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14049647 | HCID 14049647 | 52% |
Reaction Steps
A 5.00 g quantity of 5-chloro-4-hydroxy-2-pyridone and 3.66 ml of acetyl chloride were stirred in 250 ml of pyridine at room temperature for 3 hours. The reaction mixture was then concentrated and the concentrate was washed with ethyl acetate and water to produce 3.39 g of the title compound in a yield of 52%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-ac4372b4a3d243bcb68fec4e31af3e20 |
| Source note | uspto-grants-1992_10 |