HuagongsheHuagongshe Chemistry Print Report · For research reference only
Valeryl chloride → HCID 14049622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | HCID 21819823 | HCID 21819823 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14049622 | HCID 14049622 | 18% |
Reaction Steps
The general procedure of Example 27 was repeated using 1.00 g of 2,4-bis(trimethylsilyloxy)-pyridine, 50 ml of dichloromethane, 1.02 ml of pentanoyl chloride and 0.10 ml of stannic chloride, thereby producing 200 mg of the title compound in a yield of 18%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-34d1c4e3c68848ce97414a6baac95f68 |
| Source note | uspto-grants-1992_10 |