HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 54738692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 4-Hydroxy-2(1H)-pyridinone | HCID 54696004 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54738692 | HCID 54738692 | 30% |
Reaction Steps
A 0.64 ml quantity of methyl isocyanate was added to a suspension of 1.00 g of 4-hydroxy-2-pyridone in 20 ml of pyridine and the mixture was stirred at room temperature for one hour. Thereafter the general procedure of Example 36 was followed to produce the title compound in a yield of 30%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-45181d468ecc408183419b6cdb8902f6 |
| Source note | uspto-grants-1992_10 |