HRID466139

反应详情

EQUATION

反应方程式

HRID 466139 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A 2.14 g quantity of 4-n-propoxybenzoyl chloride was added to a suspension of 1.00 g of 4-hydroxy-2-pyridone in 30 ml of pyridine, and the mixture was stirred at room temperature for 4 hours. The reaction mixture was concentrated and the concentrate was washed with ethyl acetate and water, thereby producing 1.98 g of the title compound in a yield of 81%.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated
  2. washthe concentrate was washed with ethyl acetate and water