HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Propoxybenzoyl chloride → HCID 14049672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Propoxybenzoyl chloride | HCID 12434574 | — |
| Reactant | 4-Hydroxy-2(1H)-pyridinone | HCID 54696004 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14049672 | HCID 14049672 | 81% |
Reaction Steps
A 2.14 g quantity of 4-n-propoxybenzoyl chloride was added to a suspension of 1.00 g of 4-hydroxy-2-pyridone in 30 ml of pyridine, and the mixture was stirred at room temperature for 4 hours. The reaction mixture was concentrated and the concentrate was washed with ethyl acetate and water, thereby producing 1.98 g of the title compound in a yield of 81%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-79dee03760b649ff9ad218c715f1372a |
| Source note | uspto-grants-1992_10 |