HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 14049603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178475520 | HCID 178475520 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 14049603 | HCID 14049603 | 96% |
Reaction Steps
The general procedure of Example 21 was followed using 200 mg of 2-acetoxy-5-chloro-4-hydroxypyridine, 0.15 ml of benzoyl chloride and 0.74 ml of triethylamine and 20 ml of acetonitrile, thereby giving 300 mg of the title compound in a yield of 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-58ddfc3ee6b044f7a436644cc9ffef0d |
| Source note | uspto-grants-1992_10 |