HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 14049687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 54734184 | HCID 54734184 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14049687 | HCID 14049687 | 93% |
Reaction Steps
The general procedure of Example 49 was followed using 200 mg of 5-chloro-1-ethoxymethyl-4-hydroxy-2-pyridone, 0.14 ml of benzoyl chloride, 0.68 ml of triethylamine and 20 ml of dioxane, thereby producing 280 mg of the title compound in a yield of 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-e6f766f92ac9417a9ee7f0f7b50cae28 |
| Source note | uspto-grants-1992_10 |