HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenecarbonyl chloride → HCID 14049610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenecarbonyl chloride | HCID 70146 | — |
| Reactant | Gimeracil | HCID 54679224 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14049610 | HCID 14049610 | 81.9% |
Reaction Steps
The general procedure of Example 45 was followed using 2.00 g of 5-chloro-4-hydroxy-2-pyridone, 3.93 g of α-naphthoyl chloride and 100 ml of pyridine, thereby producing 3.83 g of the title compound in a yield of 61%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-dddd551d659c4d85a9973704360f446b |
| Source note | uspto-grants-1992_10 |