2,4-Dichlorobenzoyl chloride → HCID 178524393, compound

HRID 466168Notes

Reaction equation

HRID 466168 reaction equation
Cl.[OH:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([OH:9])[N:4]=1.[Cl:10][C:11]1[CH:19]=[C:18]([Cl:20])[CH:17]=[CH:16][C:12]=1[C:13](Cl)=[O:14]>>[Cl:10][C:11]1[CH:19]=[C:18]([Cl:20])[CH:17]=[CH:16][C:12]=1[C:13]([O:9][C:5]1[N:4]=[C:3]([OH:2])[CH:8]=[CH:7][CH:6]=1)=[O:14]

Participants

3

Reactant 2

HCID 666452,4-Dichlorobenzoyl chlorideHCID 178479628HCID 178479628, compound

Product 1

HCID 178524393HCID 178524393, compoundYield 78%

Procedure

The general procedure of Example 81 was followed using 3.00 g of 2,6-dihydroxypyridine hydrogen-chloride and 4.26 g of 2,4-dichlorobenzoyl chloride, thereby producing 4.49 g of the title compound in a yield of 78%.

Sources & evidence

ORD record
ord-65bac1bec94b4eb2a00e3228b5e03b4b
Source dataset
uspto-grants-1992_10
Patent number
US05155113

Reaction notes

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