Bromine → HCID 18941092, compound

HRID 46631Notes

Reaction equation

HRID 46631 reaction equation
[CH3:1][CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[CH2:4][CH2:3]1.[Br:13]Br>C(OCC)(=O)C>[Br:13][CH:4]1[CH2:3][CH:2]([CH3:1])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]1=[O:12]

Participants

4

Reactant 2

HCID 24408BromineHCID 892321,2,3,4-Tetrahydro-4-methylnaphthalen-1-one

Product 1

HCID 18941092HCID 18941092, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

4.8 g (0.03 mole) of 4-methyl-1-tetralone are reacted with 4.8 g (0.03 mole) of bromine in ethyl acetate, analogously to the instructions indicated in Example 29 (a), to give 2-bromo-4-methyl-1-tetralone. The oily product is further processed immediately without further purification.

Sources & evidence

ORD record
ord-98e49131877e4a4cbc5dc8fb849bd8e0
Source dataset
uspto-grants-1979_11
Patent number
US04174397

Reaction notes

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