HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Bromo-6-chloro-1-tetralone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 6-Chloro-1-tetralone | HCID 12291149 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Bromo-6-chloro-1-tetralone | HCID 20386488 | — |
Reaction Steps
5 g of 6-chloro-1-tetralone are reacted with 4.4 g of bromine in ethyl acetate analogously to the instructions indicated in Example 29 (a). After distilling off the solvent under reduced pressure, 2-bromo-6-chloro-1-tetralone is obtained as an amorphous residue, which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04174397 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-9afeabfb0de946a896d15fcb22c8c879 |
| Source note | uspto-grants-1979_11 |