HRID46640

反应详情

EQUATION

反应方程式

HRID 46640 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

20-Deoxynarasin sodium salt (200 mg) was dissolved in ethyl acetate (10 ml). This solution was washed with 0.1 N HCl (10 ml) and then twice with water (5 ml). The resulting organic layer was evaporated to dryness to give a residue which was redissolved in dioxane and lyophilized to give 139.6 mg of 20-deoxynarasin free acid as a white solid.

WORKUP

后处理

  1. washThis solution was washed with 0.1 N HCl (10 ml)
  2. customThe resulting organic layer was evaporated to dryness
  3. customto give a residue which