HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178439966, compound → HCID 178439984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178439966 | HCID 178439966 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178439984 | HCID 178439984 | — |
Reaction Steps
6-Chloro-8-propyl-9-(2'-(tetrazol-5-yl)biphen-4-yl)methylpurine (0.030 g) was dissolved in ethanol (2 ml) and was stirred under an atmosphere of hydrogen in presence of Pd-C(10%) (0.01 g) for 24 hours. The catalyst was filtered off and the filtrate was evaporated to dryness giving the pure desired product as a glass like solid (0.020 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05157026 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-65aa6e1dd5584a6d9c0cb79e0129ff5a |
| Source note | uspto-grants-1992_10 |