2,6-Dimethyl-8-ethyl-1-deazapurine → Hydrochloric Acid

HRID 466731Notes

Reaction equation

HRID 466731 reaction equation
[CH3:1][C:2]1[N:7]=[C:6]2[N:8]=[C:9]([CH2:11][CH3:12])[NH:10][C:5]2=[C:4]([CH3:13])[CH:3]=1.C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)[N:21]2[C:25]([C:26]3[C:31]([C:32]4[CH:37]=[CH:36][C:35]([CH2:38]Br)=[CH:34][CH:33]=4)=[CH:30][CH:29]=[C:28]([Cl:40])[CH:27]=3)=[N:24][N:23]=[N:22]2)C=CC=CC=1>>[CH3:1][C:2]1[N:7]=[C:6]2[N:8]([CH2:38][C:35]3[CH:34]=[CH:33][C:32]([C:31]4[CH:30]=[CH:29][C:28]([Cl:40])=[CH:27][C:26]=4[C:25]4[NH:21][N:22]=[N:23][N:24]=4)=[CH:37][CH:36]=3)[C:9]([CH2:11][CH3:12])=[N:10][C:5]2=[C:4]([CH3:13])[CH:3]=1.[ClH:40]

Participants

4

Reactant 2

HCID 98153742,6-Dimethyl-8-ethyl-1-deazapurineHCID 131717266HCID 131717266, compound

Product 2

HCID 313Hydrochloric AcidHCID 178437429HCID 178437429, compound

Procedure

The title compound was prepared from 5,7-dimethyl-2-ethylimidazo[4,5-b]pyridine and N-triphenylmethyl-5-(4'-bromomethyl-4-chlorobiphen-2-yl)tetrazole in a manner similar to Example 7, and was isolated as an HCl salt.

Sources & evidence

ORD record
ord-d5d280b96f724fadbdc2beb272ab8414
Source dataset
uspto-grants-1992_10
Patent number
US05157026

Reaction notes

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