HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178435160, compound → Ammonium Hydroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178435160 | HCID 178435160 | — |
| Reactant | HCID 178439890 | HCID 178439890 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Ammonium Hydroxide | HCID 14923 | — |
| Product | HCID 178439889 | HCID 178439889 | — |
Reaction Steps
To 10 mg of 57 in 100 λ CHCl3 in a polyethylene mini-centrifuge tube was added ~0.1 ml 48% aq. HF. The two-phase mix was vigorously stirred for two hours, then evaporated to dryness under a nitrogen stream. Preparative tlc of the residue on silica gel GF with 2:20:80 NH4OH:MeOH:CHCl3 afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05157040 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-26d131090f094fe89eeaf3804b2cc261 |
| Source note | uspto-grants-1992_10 |