HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(2-chloroethyl) ether → 1,5-Bis(4-iodophenoxy)-3-oxapentane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(2-chloroethyl) ether | HCID 8115 | — |
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 1,5-Bis(4-iodophenoxy)-3-oxapentane | HCID 19021957 | — |
Reaction Steps
A mixture prepared by adding 3.08 g of sodium hydroxide and 40 ml of n-butanol to 15.4 g of 4-iodophenol was refluxed. 2 ml of n-butanol solution of 5.01 g of 1,5-dichloro-3-oxapentane was added dropwise to the above prepared mixture over a period of 5 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158850 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-e2c411fd6c3544b8a2d1799b7d87fe83 |
| Source note | uspto-grants-1992_10 |