Cyclohexylamine → HCID 15233410, compound

Participants

Reaction Steps

A solution of isoproyl 2-(1,3-dithiol-2-ylidene)-2-(pivaloyloxycarbonyl)acetate (13.2 g) and cyclohexylamine (3.97 g) in methylene chloride (100ml) was stirred at room temperature for 2 hrs. The reaction mixture was washed with aqueous sodium hydroxide solution and water and then evaporated to dryness. The resultant residue was recrystallized from ethyl acetate to afford the pure product. (12.0 g, 91.6%)

Provenance & Evidence