HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 466985Generated: October 29, 2026
Anthranilic Acid → HCID 19813270, compound
https://huagongshe.com/reaction/466985
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | HCID 19813261 | HCID 19813261 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19813270 | HCID 19813270 | — |
Reaction Steps
Isopropyl 2-(1,3-dithiol-2-ylidene)-2-(ethoxycarbonyloxy-carbonyl)acetate (15.9 g) and anthranilic acid (14 dissolved in DMF (100 ml). The mixture was stirred at 60° C. for hrs. The reaction mixture was poured into ice-water. The solid formed was filtered and recrystallized from ethyl acetate to give the titled compound. (5.6 g, 30.7%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05158950 |
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| Source dataset | uspto-grants-1992_10 |
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| ORD ID | ord-152f9c6579cd44b89a96116681b901a5 |
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| Source note | uspto-grants-1992_10 |
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