HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 178517109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 178456605 | HCID 178456605 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178517109 | HCID 178517109 | 97.1% |
Reaction Steps
To a suspension of 3,4-dihydro-4-imino-3-allyl-2(1H)-quinazolinone (0.5 g, 2.5 mmol) in water (30 mL) was added N-bromosuccinimide (443 mg, 2.5 mmol). The mixture was allowed to stir at room temperature for 30 minutes. The solid was collected by filtration and washed with water (10 mL) to afford 2-bromomethyl-2,3-dihydroimidazo[1,2-c]quinazolin-5(6H)-one (680 mg, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158953 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-a0e876b5d9e34f8cbaaf9d260bd02f98 |
| Source note | uspto-grants-1992_10 |