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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 466991Generated: October 30, 2026

N-bromobutanimide → HCID 178517109, compound

https://huagongshe.com/reaction/466991

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 178456605HCID 178456605—
SolventWaterHCID 962—
ProductHCID 178517109HCID 17851710997.1%

Reaction Steps

To a suspension of 3,4-dihydro-4-imino-3-allyl-2(1H)-quinazolinone (0.5 g, 2.5 mmol) in water (30 mL) was added N-bromosuccinimide (443 mg, 2.5 mmol). The mixture was allowed to stir at room temperature for 30 minutes. The solid was collected by filtration and washed with water (10 mL) to afford 2-bromomethyl-2,3-dihydroimidazo[1,2-c]quinazolin-5(6H)-one (680 mg, 97%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05158953
Source datasetuspto-grants-1992_10
ORD IDord-a0e876b5d9e34f8cbaaf9d260bd02f98
Source noteuspto-grants-1992_10