HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Benzyl-N-ethyl-4-methanesulphonamidophenethylamine → N-Ethyl-4-methanesulphonamidophenethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Benzyl-N-ethyl-4-methanesulphonamidophenethylamine | HCID 19813439 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-Ethyl-4-methanesulphonamidophenethylamine | HCID 17890649 | — |
Reaction Steps
N-Benzyl-N-ethyl-4-methanesulphonamidophenethylamine (4.3 g, 12.9 mmole) was stirred under a hydrogen atmosphere (50 p.s.i.=344.7 kPa) in ethanol (50 ml) containing 10% Pd/C (0.5 g) for 5 hours. The mixture was then filtered, evaporated and the residue triturated with ether to give the title compound, yield 2.6 g, m.p. 125°-128°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158964 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-fa74015620eb47dc8eb12f2b170f6d55 |
| Source note | uspto-grants-1992_10 |