HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18648568, compound → HCID 53977342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18648568 | HCID 18648568 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53977342 | HCID 53977342 | — |
Reaction Steps
1.1 g of N-(1-carboethoxy-3-benzoxycarbonylaminopropyl)-L-alanyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid are dissolved in 150 ml of methanol and are hydrogenated in the presence of 100 mg of palladium/active charcoal (10% strength) at 40° C. under normal pressure. After the end of the reaction, the solution is filtered off from the catalyst and the solvent is stripped off in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158959 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-ab7d83664b554e1e8b6f7cf8cf97a7bf |
| Source note | uspto-grants-1992_10 |