HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14210337, compound → HCID 7408314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14210337 | HCID 14210337 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 7408314 | HCID 7408314 | — |
Reaction Steps
7.0 g Boc-Phe-Gly-Gly-OBzl was reduced in the presence of Pd-black as a catalyst in 200 ml MeOH, and this was followed by concentration. The resulting concentrate, after the addition of 1.72 ml CHA, was crystallized with AcOEt and collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05159061 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-8fd757bea52a4a1cb12db51f1edcb258 |
| Source note | uspto-grants-1992_10 |