HCID 46221559, compound → 5-Cyclohexyl-2-propylpentan-1-ol

HRID 467396Notes

Reaction equation

HRID 467396 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]([CH2:13][CH2:14][CH3:15])[CH2:11][OH:12])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H][H]>>[CH:1]1([CH2:7][CH2:8][CH2:9][CH:10]([CH2:13][CH2:14][CH3:15])[CH2:11][OH:12])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 46221559HCID 46221559, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 202790005-Cyclohexyl-2-propylpentan-1-olYield 98.2%

Procedure

365 g of 5-Phenyl-2-n-propyl-pentanol of Synthesis Example 1.2 were combined with 10 g Ru on activated carbon (Ru content: 5 wt. %) and hydrogenated at a hydrogen pressure of 20 bar and at a temperature of 120° C. After 5-7 hours the reaction was finished. The catalyst was removed and the product distilled. 345 g (content: 98.2%) of 5-cyclohexyl-2-n-propyl-pentanol are obtained. Yield: 90.8% of theoretical.

Workup

  1. customThe catalyst was removed
  2. distillationthe product distilled

Sources & evidence

ORD record
ord-d86b904b2608445ea1114f5a65475e79
Source dataset
uspto-grants-2014_01
Patent number
US08623340B2

Reaction notes

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