HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46221559, compound → 5-Cyclohexyl-2-propylpentan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46221559 | HCID 46221559 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | 5-Cyclohexyl-2-propylpentan-1-ol | HCID 20279000 | 98.2% |
Reaction Steps
365 g of 5-Phenyl-2-n-propyl-pentanol of Synthesis Example 1.2 were combined with 10 g Ru on activated carbon (Ru content: 5 wt. %) and hydrogenated at a hydrogen pressure of 20 bar and at a temperature of 120° C. After 5-7 hours the reaction was finished. The catalyst was removed and the product distilled. 345 g (content: 98.2%) of 5-cyclohexyl-2-n-propyl-pentanol are obtained. Yield: 90.8% of theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623340B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-d86b904b2608445ea1114f5a65475e79 |
| Source note | uspto-grants-2014_01 |