HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylisohexanol → 3-Methyl-5-cyclohexylpentanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylisohexanol | HCID 108312 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | 3-Methyl-5-cyclohexylpentanol | HCID 21267766 | 99.7% |
Reaction Steps
1200 g of 3-Methyl-5-phenyl-pentanol (Phenoxanol™, supplier: IFF) combined with 10.5 g Ru on aluminium oxide (Ru content 5 wt. %) were hydrogenated at a hydrogen pressure of 25 bar and at a temperature of 110° C. After 15 hours the reaction was finished. The catalyst was removed and the product distilled. 1204 g (content 99.7%) of 5-cyclohexyl-3-methyl-pentanol were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623340B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-74245e376ce243d8bf55cd9d2d5c3841 |
| Source note | uspto-grants-2014_01 |