Potassium Carbonate → HCID 70922455, compound

Participants

Reaction Steps

1.5 g of K2CO3 is added to a solution of 1.15 g of the compound from step 1 in 40 ml of MeOH/THF mixture (50/50; v/v) and stirred for 4 hours at RT. The reaction mixture is concentrated under vacuum, the residue is taken up in EtOAc/water mixture, the organic phase is washed with water, with saturated NaCl solution, dried over Na2SO4 and the solvent is evaporated under vacuum. The residue is taken up in iso ether and the precipitate that formed is drained. 0.9 g of the expected compound is obtained.

Provenance & Evidence