反应详情

Compounds 6 (3 g, 13.18 mmole) and 17 (3.9 g, 13.18 mmole) were combined in CH3CN (25 mL) and heated for one hr. Mass spectroscopy indicated no starting material. Saturated K2CO3 was added and the reaction was extracted 3× with EtOAc. The organic layers were combined, washed with brine and concentrated in vacuo to give 6.48 g of 7 (78.4%).

1. temperatureheated for one hr
2. extractionthe reaction was extracted 3× with EtOAc
3. washwashed with brine
4. concentrationconcentrated in vacuo