HRID46795

反应详情

EQUATION

反应方程式

HRID 46795 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Butyl glycidyl ether (232.5 g), 2,2-bis(p-hydroxyphenyl)propane (171 g), and benzyltrimethylammonium chloride (4 g) were stirred and heated slowly to 100°. The mixture was kept at 100° for 1 hour, then at 110° for 2 hours, 120° for 1 hour, and 150° for 11/2 hours. The product had an epoxy value of 0.2 equiv./kg.

WORKUP

后处理

  1. temperatureheated slowly to 100°
  2. waitat 110° for 2 hours
  3. wait120° for 1 hour
  4. custom150°
  5. custom2 hours