HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → 4-Amino-6-(1-methylcyclopropyl)-3-methylthio-1,2,4-triazin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 178421680 | HCID 178421680 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 4-Amino-6-(1-methylcyclopropyl)-3-methylthio-1,2,4-triazin-5-one | HCID 20488920 | 82.3% |
Reaction Steps
198 grams of the compound obtained according to (b) were dissolved in 500 ml of 2 normal NaOH and treated with 500 ml of methane and 150 grams of methyl iodide. The mixture was stirred for 6 hours at 20° to 30° C. The crystals formed were filtered off with suction, washed and dried. There are obtained 174.5 grams of final product (dried in a vacuum at 40° C.), white crystals, M.P. 115° to 116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04175188 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-5466c7e1b96f44aa85af8215829ebd59 |
| Source note | uspto-grants-1979_11 |