HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Diiodohexane → 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione}
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Diiodohexane | HCID 12373 | — |
| Reactant | 1,1'-Butane-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763837 | — |
| Product | 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763838 | 27% |
Reaction Steps
The experimental protocol used is the same as that described for the synthesis of the compound of Example 1, 1,6-diiodohexane replacing 1,4-dibromobutane. The expected compound is obtained in the form of a light yellow solid with a yield of 27%. Melting point: 187-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08624037B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-3ea8d0c5a6b24f7daeb679b1c6c2cb68 |
| Source note | uspto-grants-2014_01 |