HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,4-Dichloro-cis-2-butene → 1,1'-(2z)-But-2-ene-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione}
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,4-Dichloro-cis-2-butene | HCID 6432115 | — |
| Edukt | 1,1'-Butane-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763837 | — |
| Produkt | 1,1'-(2z)-But-2-ene-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 87135216 | 40% |
Reaktionsschritte
The experimental protocol used is the same as that described for the synthesis of the compound of Example 1, cis-1,4-dichloro-2-butene replacing 1.4 dibromobutane. The expected compound is obtained in the form of a pale yellow solid with a yield of 40%. Melting point: 191-193° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08624037B2 |
| Quelldatensatz | uspto-grants-2014_01 |
| ORD ID | ord-4b2fe6b5a50044c2aca6c0af38ce7a54 |
| Quellennotiz | uspto-grants-2014_01 |