HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 46175543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 1-[3-(pyrrolidin-1-yl)propyl]-1,4-diazepane | HCID 2737251 | — |
| Reactant | HCID 58393320 | HCID 58393320 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 46175543 | HCID 46175543 | — |
Reaction Steps
The title compound was prepared according to general procedure AA using 5-({[(4-bromo-2-ethylphenyl)sulfonyl](methyl)amino}methyl)furan-3-carboxylic acid (50 mg, 0.12 mmol), CDI (41 mg, 0.25 mmol) and 1-[3-(pyrrolidin-1-yl)propyl]-1,4-diazepane (53 mg, 0.25 mmol) in DCE (2 mL). The crude product was purified using prep method A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623859B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-d5f66385393c45dc923593333fbfa5ec |
| Source note | uspto-grants-2014_01 |