HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 46175542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 1-{3-[(Pyrrolidin-1-yl)methyl]phenyl}methanamine | HCID 4712478 | — |
| Reactant | HCID 58393320 | HCID 58393320 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 46175542 | HCID 46175542 | — |
Reaction Steps
The title compound was prepared according to general procedure AA using 5-({[(4-bromo-2-ethylphenyl)sulfonyl](methyl)amino}methyl)furan-3-carboxylic acid (40 mg, 0.10 mmol), CDI (32 mg, 0.2 mmol) and 1-[3-(pyrrolidin-1-ylmethyl)phenyl]methanamine (57 mg, 0.3 mmol) in DCE (2 mL). The crude product was purified using prep method A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623859B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-e11fe79c16e94755835cdab50ff90f6d |
| Source note | uspto-grants-2014_01 |