HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 58393372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86762214 | HCID 86762214 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58393372 | HCID 58393372 | — |
Reaction Steps
tert-butyl (2-{4-[(3aR,7aR)-octahydro-1H-benzimidazol-2-yl]phenyl}ethyl)carbamate (50 mg, 0.15 mmol) was stirred in a 4:1 mixture of DCM:TFA (1 mL) at ambient temperature for 18 h. The reaction was concentrated in vacuo and the crude product used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623859B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-0f462ca0f42e4e428b660eb1b2bed395 |
| Source note | uspto-grants-2014_01 |