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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469303Generated: October 27, 2026

Bms-973013 → HCID 58181131, compound

https://huagongshe.com/reaction/469303

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBms-973013HCID 22293182—
Reactant(4-Benzyloxy-3,5-dimethyl-phenyl)-(6-chloro-pyrimidin-4-yl)-methanoneHCID 58181140—
SolventDimethylformamideHCID 6228—
ProductHCID 58181131HCID 58181131—

Reaction Steps

170 mg (0.779 mmol) 1-piperidin-4-yl-1,3-dihydro-imidazo[4,5-b]pyridin-2-one, 270 mg (0.727 mmol) (4-benzyloxy-3,5-dimethyl-phenyl)-(6-chloro-pyrimidin-4-yl)-methanone and 0.200 mL (1.42 mmol) TEA were combined in 2.0 mL DMF and stirred overnight at RT. The reaction mixture was stirred into ice water, the precipitate was suction filtered and dried.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629137B2
Source datasetuspto-grants-2014_01
ORD IDord-3e22de6a59f8487f849ddb4b6c9ea5bb
Source noteuspto-grants-2014_01