HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bms-973013 → HCID 58181131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bms-973013 | HCID 22293182 | — |
| Reactant | (4-Benzyloxy-3,5-dimethyl-phenyl)-(6-chloro-pyrimidin-4-yl)-methanone | HCID 58181140 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58181131 | HCID 58181131 | — |
Reaction Steps
170 mg (0.779 mmol) 1-piperidin-4-yl-1,3-dihydro-imidazo[4,5-b]pyridin-2-one, 270 mg (0.727 mmol) (4-benzyloxy-3,5-dimethyl-phenyl)-(6-chloro-pyrimidin-4-yl)-methanone and 0.200 mL (1.42 mmol) TEA were combined in 2.0 mL DMF and stirred overnight at RT. The reaction mixture was stirred into ice water, the precipitate was suction filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629137B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-3e22de6a59f8487f849ddb4b6c9ea5bb |
| Source note | uspto-grants-2014_01 |