HRID469337

反应详情

EQUATION

反应方程式

HRID 469337 的结构方程式

PROCEDURE

实验过程

1.63 g (10.00 mmol) 3,5-difluoro-benzoic acid were mixed with 20 mL thionyl chloride and boiled for 2 h. The reaction mixture was evaporated to dryness and coevaporated twice with toluene. The residue was reacted further as the crude product.

WORKUP

后处理

  1. customThe reaction mixture was evaporated to dryness
  2. customThe residue was reacted further as the crude product