Ethyl 3-aminobenzoate → HCID 67124900, compound

Participants

Reaction Steps

To a solution of benzo[b]thiophen-3-ylboronic acid (500 mg, 2.81 mmol) and 2-oxoacetic acid hydrate (259 mg, 2.81 mmol) in acetonitrile (20 ml), was added ethyl 3-aminobenzoate (419 μl, 2.81 mmol). The reaction was stirred at r.t. for 72 hours, and then the solvent was evaporated under vacuum. The residue was used in the next step without any further purification.

Provenance & Evidence