HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 53237281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 67160580 | HCID 67160580 | — |
| Product | HCID 53237281 | HCID 53237281 | — |
Reaction Steps
The product from Example 19A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 3.77 (s, 2H) 7.06-7.22 (m, 3H) 7.98-8.20 (m, 3H) 8.37 (d, J=7.32 Hz, 1H) 11.82 (s, 1H); MS (ESI) m/z 350 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-a297b2266239448fae0b7ae9bbcf6b1f |
| Source note | uspto-grants-2014_01 |