HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chlorophenyl)acetic acid → HCID 53237495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chlorophenyl)acetic acid | HCID 15880 | — |
| Reactant | HCID 67160099 | HCID 67160099 | — |
| Product | HCID 53237495 | HCID 53237495 | — |
Reaction Steps
The product from Example 22B and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 0.79-0.92 (m, 2H) 0.92-1.07 (m, 2H) 2.45-2.55 (m, 1H) 3.67 (s, 2H) 7.32-7.52 (m, 4H) 7.92 (t, J=8.09 Hz, 1H) 7.99-8.14 (m, 1H) 8.31 (t, J=7.32 Hz, 2H) 11.50 (s, 1H); MS (ESI) m/z 354 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-3bca79519107420c9a10cc7556a3645f |
| Source note | uspto-grants-2014_01 |