3,5-Difluorophenylacetic acid → HCID 53237498, compound

Participants

Reaction Steps

The product from Example 22B and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 0.79-0.94 (m, 2H) 0.93-1.09 (m, 2H) 2.42-2.55 (m, 1H) 3.73 (s, 2H) 6.95-7.29 (m, 3H) 7.92 (t, J=7.63 Hz, 1H) 7.98-8.13 (m, 1H) 8.32 (d, J=7.93 Hz, 2H) 11.56 (s, 1H); MS (ESI) m/z 356 (M+H)+.

Provenance & Evidence