HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chlorophenyl)acetic acid → HCID 53237737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chlorophenyl)acetic acid | HCID 15880 | — |
| Reactant | 2-Amino-4-methyl-1(2H)-phthalazinone | HCID 819574 | — |
| Product | HCID 53237737 | HCID 53237737 | — |
Reaction Steps
The product from Example 28A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 2.54 (s, 3H) 3.74 (s, 2H) 6.94-7.09 (m, 1H) 7.10-7.20 (m, 3H) 7.85-7.98 (m, 1H) 7.95-8.11 (m, 2H) 8.32 (d, J=7.93 Hz, 1H) 11.47-11.69 (m, 1H); MS (ESI) m/z 328 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-bd2b7bd4664c4288a6329953cccd6dc6 |
| Source note | uspto-grants-2014_01 |