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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469540Generated: October 30, 2026

(4-Chlorophenyl)acetic acid → HCID 53237737, compound

https://huagongshe.com/reaction/469540

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(4-Chlorophenyl)acetic acidHCID 15880—
Reactant2-Amino-4-methyl-1(2H)-phthalazinoneHCID 819574—
ProductHCID 53237737HCID 53237737—

Reaction Steps

The product from Example 28A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 2.54 (s, 3H) 3.74 (s, 2H) 6.94-7.09 (m, 1H) 7.10-7.20 (m, 3H) 7.85-7.98 (m, 1H) 7.95-8.11 (m, 2H) 8.32 (d, J=7.93 Hz, 1H) 11.47-11.69 (m, 1H); MS (ESI) m/z 328 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-bd2b7bd4664c4288a6329953cccd6dc6
Source noteuspto-grants-2014_01