HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-cyclobutylacetic Acid → HCID 53238205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-cyclobutylacetic Acid | HCID 1516411 | — |
| Reactant | 2-amino-4-(trifluoromethyl)phthalazin-1(2H)-one | HCID 67161111 | — |
| Product | HCID 53238205 | HCID 53238205 | — |
Reaction Steps
The product of Example 11B and 2-cyclobutylacetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO) δ 11.61-11.40 (m, 1H), 8.46-8.38 (m, 1H), 8.17-8.09 (m, 1H), 8.09-7.98 (m, 2H), 2.73-2.61 (m, 1H), 2.46 (d, J=7.5, 2H), 2.15-2.01 (m, 2H), 1.93-1.70 (m, 4H); MS (ESI) m/z 326 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-119a74f2492847b6a81d2ffe9df5743a |
| Source note | uspto-grants-2014_01 |