2-Thiopheneacetyl chloride → HCID 67160795, compound

Participants

Reaction Steps

The product of Example 11B and 2-(thiophen-2-yl)acetyl chloride were treated using a method similar to that described in Example 53 to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.88-11.97 (m, 1H), 8.41-8.48 (m, 1H), 8.13 (td, J=7.7, 1.6 Hz, 1H), 8.00-8.09 (m, 2H), 7.43 (dd, J=5.1, 1.3 Hz, 1H), 7.04-7.08 (m, 1H), 7.01 (dd, J=5.1, 3.5 Hz, 1H), 3.96 (d, J=0.9 Hz, 2H); MS (ESI−) M/Z 352 (M−H)−.

Provenance & Evidence