HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5-methylthiophen-2-yl)acetic Acid → HCID 67161151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5-methylthiophen-2-yl)acetic Acid | HCID 4527177 | — |
| Reactant | 2-amino-4-(trifluoromethyl)phthalazin-1(2H)-one | HCID 67161111 | — |
| Product | HCID 67161151 | HCID 67161151 | — |
Reaction Steps
The product of Example 11B and 2-(5-methylthiophen-2-yl)acetic acid were treated using a method similar to that described in Example 5 to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.85-11.96 (m, 1H), 8.43 (d, J=6.9 Hz, 1H), 8.10-8.17 (m, 1H), 8.01-8.08 (m, 2H), 6.81 (d, J=3.4 Hz, 1H), 6.66-6.68 (m, 1H), 3.84-3.85 (bs, 2H), 2.41 (d, J=0.8 Hz, 3H); MS (ESI+) M/Z 368 (M+H)+, 385 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-1baf0b0201ea42b0aba12109e9460b39 |
| Source note | uspto-grants-2014_01 |