Cyclopentylacetic acid → HCID 67160272, compound

Participants

Reaction Steps

The product from Example 62A and 2-cyclopentylacetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.18 (s, 1H), 8.39 (d, J=2.0 Hz, 2H), 7.93-8.00 (m, 1H), 7.87 (t, J=7.5 Hz, 1H), 2.20-2.31 (m, 3H), 1.74-1.90 (m, 2H), 1.47-1.70 (m, 4H), 1.47 (s, 9H), 1.17-1.33 (m, 2H); MS (ESI+) M/Z 328 (M+H)+.

Provenance & Evidence