4-Chlorophenylacetyl chloride → HCID 67160101, compound

Participants

Reaction Steps

The product from Example 62A and 2-(4-chlorophenyl)acetyl chloride were treated using a method similar to that described in Example 1C to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.54 (s, 1H), 8.38 (d, J=8.3 Hz, 1H), 8.37 (dd, J=7.7, 1.6 Hz, 1H), 7.94-8.00 (m, 1H), 7.84-7.90 (m, 1H), 7.41 (s, 4H), 3.68 (s, 2H), 1.47 (s, 9H); MS (ESI+) M/Z 370 (M+H)+.

Provenance & Evidence