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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469580Generated: October 31, 2026

3,5-Difluorophenylacetic acid → HCID 67161040, compound

https://huagongshe.com/reaction/469580

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 67162274HCID 67162274—
ProductHCID 67161040HCID 67161040—

Reaction Steps

The product of Example 67A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 11.62 (s, 1H), 8.35-8.28 (m, 1H), 8.01-7.94 (m, 1H), 7.94-7.85 (m, 2H), 7.20-7.10 (m, 3H), 4.12-3.99 (m, 1H), 3.76 (s, 2H), 2.42-2.22 (m, 4H), 2.14-2.00 (m, 1H), 1.89-1.76 (m, 1H); MS (ESI) m/z 370 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-0ee075cdc3e44315aa7d03880038c676
Source noteuspto-grants-2014_01