HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chlorophenyl)acetic acid → HCID 67160473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chlorophenyl)acetic acid | HCID 15880 | — |
| Reactant | HCID 67161381 | HCID 67161381 | — |
| Product | HCID 67160473 | HCID 67160473 | — |
Reaction Steps
The product of Example 71A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.52-11.54 (bs, 1H), 8.31 (dd, J=7.9, 1.3 Hz, 1H), 8.13 (d, J=8.1 Hz, 1H), 7.97-8.02 (m, 1H), 7.87-7.91 (m, 1H), 7.35-7.47 (m, 4H), 3.62-3.77 (m, 3H), 1.96-2.10 (m, 2H), 1.59-1.87 (m, 6H); MS (ESI) m/z 382 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-e5e14d2ff432462faf989d2f57d1eff7 |
| Source note | uspto-grants-2014_01 |