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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469583Generated: October 31, 2026

3,5-Difluorophenylacetic acid → HCID 67160414, compound

https://huagongshe.com/reaction/469583

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 67161381HCID 67161381—
ProductHCID 67160414HCID 67160414—

Reaction Steps

The product of Example 71A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.58-11.61 (bs, 1H), 8.33 (dd, J=7.9, 1.3 Hz, 1H), 8.14 (d, J=8.1 Hz, 1H), 7.98-8.02 (m, 1H), 7.87-7.92 (m, 1H), 7.09-7.22 (m, 3H), 3.74-3.75 (m, 2H), 3.70 (d, J=7.8 Hz, 1H), 1.97-2.11 (m, 2H), 1.59-1.94 (m, 6H); MS (ESI) m/z 384 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-279a061293c5455db1abb7b8d61c52e6
Source noteuspto-grants-2014_01