HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 67160414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 67161381 | HCID 67161381 | — |
| Product | HCID 67160414 | HCID 67160414 | — |
Reaction Steps
The product of Example 71A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.58-11.61 (bs, 1H), 8.33 (dd, J=7.9, 1.3 Hz, 1H), 8.14 (d, J=8.1 Hz, 1H), 7.98-8.02 (m, 1H), 7.87-7.92 (m, 1H), 7.09-7.22 (m, 3H), 3.74-3.75 (m, 2H), 3.70 (d, J=7.8 Hz, 1H), 1.97-2.11 (m, 2H), 1.59-1.94 (m, 6H); MS (ESI) m/z 384 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-279a061293c5455db1abb7b8d61c52e6 |
| Source note | uspto-grants-2014_01 |