HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-2-phenylacetyl chloride → HCID 53239330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-2-phenylacetyl chloride | HCID 14949528 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 53239330 | HCID 53239330 | — |
Reaction Steps
The product of Example 86A and 2-fluoro-2-phenylacetyl chloride were treated using a method similar to that described in Example 1C to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 12.22 (s, 1H), 8.39-8.45 (m, 1H), 7.90-8.07 (m, 2H), 7.69-7.78 (m, 1H), 7.61-7.68 (m, 6H), 7.46-7.53 (m, 3H), 6.26 (d, J=47.1 Hz, 1H); MS (ESI+) M/Z 408 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-c133aa86c1c04aed981e060a1a520698 |
| Source note | uspto-grants-2014_01 |